Teadus - ja arendustegevuse erandi kohaldamine teenuse tellimisel KONTROLL-LEHT Tellitava teenuse nimetus: Fosforiidi geokeemilised uuringud Teenuse eeldatav maksumus: 13 400 eurot Teenuse lühikirjeldus (eesmärk, oodatavad tulemused, peamised tegevused): EGT teostab fosforiidi ja graptoliitargilliidi geokeemilisi uuringuid, mille käigus kontrollitakse kivimi kohta kehtivaid ajaloolistest allikatest teadaolevaid fakte ning hangitakse uus kogum geokeemilisi andmeid. Laboratoorselt määratakse fosforiidis peamised oksiidid ja floor XRF meetodil, jälgelemendid (sh haruldased muldmetallid) ICP-MS meetodil, üldväävel ja süsinik LECO instrumendiga ning raskmetallid ICP-AES meetodil. Teenuse CPV-kood ( val ida sobiv): 73000000-2 Uurimis- ja arendusteenused ja seonduvad nõustamisteenused 73111000-3 Uurimislaborite teenused. Vastavus Frascat’i manuali kriteeriumitele uudsus: Tellitav analüüside komplekt võimaldab saada süstemaatilist infot eesti fosforiidis levivate haruldaste muldmetallide jaotuse kohta. Samuti saame uut infot fosfori sisalduse kohta, mis v õimaldab valideerida ajaloolise andmestiku p õhjal koostatud ruumimudelit. loomingulisus: Erinevate meetodite kasutamine, nende kombineerimine ja tulemuste tõlgendamine on muuhulgas ka loominguline töö. Saadud tulemused on aluseks fosforiidi kvaliteedi ruumimudeli valideerimisel. tulemuste ettemääramatus: Teenus võimaldab saada Eesti fosforiidi osas uut ja süstemaatilist infot haruldaste muldmetallide ja fosfori leviku osas. Fosfori osas on üpris tihe proovivõrk juba olemas kui d tähapäeval on võimalik teha täpsemaid mõõtmisi, sest laborivõimekus on aastatega paranenud . Laboritulemuste osas ei ole tulemused ette teada. süstemaatilisus: Analüüsimine on vaieldamatult süstemaatiline , selle aluseks on juba proovide võtmise ja valimise eesmärgipärane süsteemsus . Puursüdamike uurimisprotsess, sealhulgas kivimintervallide kirjeldamine ja analüüsitavate prooviintervallide määramine on põhjalikult dokumenteeritud. ülekantavus ja/või korratavus: Selleks, et analüüside tulemused oleksid korratavad, ongi vajalik eelnimetatud teenuse d telli d a tunnustatud ja akrediteeritud uurimislaboritelt, mis tagab analüüside puhtuse, kvaliteedi ning katseparameetrite nõuetekohase kirjelduse. Oluline on ka analüüside võrreldavus varem tehtud analüüsidega graptoliitargilliidist , mille puhul kasutati sama labori teenuseid. Kasutatud kivimmaterjal arhiveeritakse edasisteks uuringuteks või kontrollanalüüside läbiviimiseks ning jääb ligipääsetavaks huvilistele. Teenused ei ole pärast uuringute läbiviimist hankija ja pakkuja vahelise hankelepingu alusel turustatavad (jah/ei): JAH Teenuste tulemustest tuleneb kasu üksnes EGT’le tema enda tegevuseks (jah/ei): EI Teenuste eest tasub täies ulatuses EGT (jah/ei): JAH Kontroll-lehe täitja nimi ja ametikoht Lauri Joosu vanemgeoloog /allkirjastatud digitaalselt/
Saatja: Lauri Joosu </o=Majandus-Teede-Sideministeerium/ou=Exchange Administrative Group (FYDIBOHF23SPDLT)/cn=Recipients/cn=9d99dc0583ce49c481de011f0>
Saaja: 'David Berglund', Kaija Laatikainen, Tiit Kaasik
Teema: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Thank You David.
I will inform you that we accept the offer. We plan to ship samples from Estonia 19th of May. If we have confirmation from logistic company and estimated time of delivery I will let you know.
All the best,
Lauri
From: David Berglund <
[email protected]>
Sent: kolmapäev, 12. mai 2021 13:08
To: Lauri Joosu <
[email protected]>; Kaija Laatikainen <
[email protected]>
Cc: Tiit Kaasik <
[email protected]>
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Hi Lauri,
That’s included in the price.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Area
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Wednesday, 12 May 2021 11:59
To: David Berglund <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Thank you this is what I need.
Please also add fluorine price to ME-XRF24. I think this was not icluded.
Lauri
From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: kolmapäev, 12. mai 2021 12:50
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Hi Lauri,
Please find attached prices.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Area
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, 11 May 2021 15:45
To: Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; David Berglund <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Hi Kaija!
I think there is some miscommunication. What I need is the estimated price (cost) for chemical analysis (request for quote) based on sample and analyse list I provided.
All the best,
Lauri
From: Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Sent: teisipäev, 11. mai 2021 16:25
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; David Berglund <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Hi Lauri,
Yes, you’ll do the proforma invoice (if needed) with the freight company you use.
PS: We have used ETS Logistics Ltd. They arranged sample shipment to us and return of samples rejects back to Geological survey of Estonia.
Contact person there is Elerin Mumm (his Mob +372 52 909 61 and email:
[email protected] <mailto:
[email protected]> ).
Regards,
Kaija
Kaija Laatikainen
Laboratory Manager, Geochemistry Outokumpu, Finland
T +358 10 470 1212
M +358 50 415 2812
[email protected] <mailto:
[email protected]>
Karjalankatu 1
FI-83 500 Outokumpu, Finland
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From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, 11 May 2021 16.06
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Hi Lauri,
Kaija can comment on that, but I think you have to do the proforma invoice with the freight company you will use.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Area
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, 11 May 2021 14:57
To: David Berglund <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Thank you for reply.
However before shipping samples I need pro forma invoice from your side can you provide this based on sample list I attatched?
Best regards,
Lauri
From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: teisipäev, 11. mai 2021 15:46
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
Hi Lauri,
Please accept my late reply.
Please find answers below in “red”.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Area
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, 11 May 2021 11:27
To: David Berglund <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >
Subject: [EXTERNAL] - RE: Price request for sample preparation and chemical analysis
CAUTION: This email originated from outside of ALS. Do not click links or open attachments unless you recognize the sender and are sure content is relevant to you.
Dear David.
I just resend the email incase you missed it.
Lauri
From: Lauri Joosu
Sent: neljapäev, 6. mai 2021 12:38
To: 'David Berglund' <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >
Subject: Price request for sample preparation and chemical analysis
Dear David.
We are now almost finished the sampling and I would like to get price proposal for sample preparation and geochemical analysis of 151 samples. Please see the sample list in attachment. In addition, I have several minor/ technical questions:
Related to sample shipping:
1. Assuming we accept price proposal we can send the samples and pay when analyses are finished?
[David Berglund] Yes, we will proceed with the sample preparation and all the analyses. When all are done we will send out the invoice.
2. How sample transportation procedure exactly works? I fill sample Submittal Form and send this this to you and add same documentation to shipment?
[David Berglund] Yes, you just need to fill in the Sample Submittal Form and send this to us and you can also add them into the shipment.
3. I have understood that sample prep is done in Finland. Please provide me the exact address, opening hours and contact phone. Is there anything else transportation company should know?
[David Berglund] Yes, we will perform all sample preparation in Outokumpu. Contact person Kaija Laatikainen,
[email protected] <mailto:
[email protected]> Open hours 8-16.
Address:
ALS Geochemistry
Karjalankatu 1
Fin-83500 Outokumpu
Finland
4. Total amount of samples is about 300 kg we are planning to use euro pallet with riser collars for shipping. Is it possible that you send back remaining samples by using the same euro pallet with riser collars? If you can send back the sample by using the same “containers”, then in future we can buy strong plastic boxes for shipping.
[David Berglund] That works fine for us.
5. Is there something else what I forgot to ask for convenient sample shipping?
[David Berglund] No
Technical questions:
1. What material is used in crusher/grinder movable parts (so I would know with which elements are samples contaminated)
[David Berglund] Please find attached what our pulverizing bowls and pucks contains.
2. What is the minimal amount of sample if we want to and standards in sample patch? In one of your previous email I understood that it was 50 g, but from 2021 lab fee .pdf fail it seems to be 10g for requested analysis?
[David Berglund] Depending on which methods you want to use, but if they also require sample preparation I would say minimum 150-200g.
3. Is it possible that you weigh remaining samples after crushing and pulverizing and provide the data when returning samples?
[David Berglund] Yes, that is now problem, we need to charge a small cost for it.
4. All samples must be analyzed in a according to sequence ID (starting from 1). If you can’t do that then please let me know.
[David Berglund] Yes, we run them in numeric order.
All the best,
Lauri Joosu
Vanemgeoloog | Maapõueressursside osakond
Senior geologist | Department of Geological Resources
[email protected] <mailto:
[email protected]> | http://www.egt.ee <https://aus01.safelinks.protection.outlook.com/?url=https%3A%2F%2Furldefense.com%2Fv3%2F__http%3A%2Fwww.egt.ee%2F__%3B!!DOxrgLBm!Q7eTg5qiVQL8VMZOpEUQ2nbP-sdBU5YrV3cWDG5jdFQlB7H1ufP-UlOMnZdGg_gLGSDBjoLCu4NX%24&data=04%7C01%7CDavid.Berglund%40alsglobal.com%7C9f63ad2c62154e39215008d9152c86ed%7C485ca04e6f7440509764cdb4bfa89c25%7C0%7C1%7C637564103910156841%7CUnknown%7CTWFpbGZsb3d8eyJWIjoiMC4wLjAwMDAiLCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C1000&sdata=XFjuv2DA2xgPSK6DwsH1ft9Eh5Jdy9lf9JU8aTl7jFU%3D&reserved=0>
Eesti Geoloogiateenistus | The Geological Survey of Estonia | F. R. Kreutzwaldi 5, 44314 Rakvere, Eesti
From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: teisipäev, 9. veebruar 2021 17:37
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi Lauri,
50g for the standards is fine.
Best rgeards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Area
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, 9 February 2021 16:26
To: David Berglund <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi.
I would like to add some in-house standards into sample stream. Material is pulverised but just not to waste it I ask if 100g is absolute minimum or eg. 50g would be also acceptable?
All the best,
Lauri
From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, February 9, 2021 3:14 PM
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Cc: ALSOT.Lab <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi Lauri,
Depending on if it´s pulps(already pulverized) its enough with 100g, but if we also should pulverize them we want if possible at least 150g.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Area
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Tuesday, 9 February 2021 13:22
To: David Berglund <
[email protected] <mailto:
[email protected]> >
Cc: ALSOT.Lab <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi David,
Can you please tell me what is the minimal sample weight for CCP-PKG3 analyse package
All the best,
Lauri
From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: Thursday, November 19, 2020 11:53 AM
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Cc: ALSOT.Lab <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi Lauri,
Thanks for your email.
F can be added into the ME-XRF24 package. Detection limit 0.1-50%.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Region
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: Wednesday, 18 November 2020 12:56
To: David Berglund <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hei.
I found another question. I understand thad Fluorine can be added to ME-XRF24 package? Please proovide analytical range and precision also for Fluorine.
All the best,
Lauri
From: Lauri Joosu
Sent: Monday, November 16, 2020 4:50 PM
To: 'David Berglund' <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Thank You for reply.
I have few follow-up questions.
1. Can you plese provide an estimate of precision (with miinimum value above it will apply) for CCP-PKG03 package and ME-ICP06 package.
2. There was comment regarding ME-MS8 „Minerals that may not recover fully using the lithium borate fusion include zircon, some metal oxides, some rare-earth phosphates and some sulphides.“ In REE-phosphates do you mean Xenotime, Monazite etc or might there be probleem if there is apatite with substitution of Ca to some REE?
All the best,
Lauri
From: David Berglund <
[email protected] <mailto:
[email protected]> >
Sent: Friday, November 13, 2020 10:15 AM
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; Johannes Vind <
[email protected] <mailto:
[email protected]> >; ALSOT.Lab <
[email protected] <mailto:
[email protected]> >; Kaija Laatikainen <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi Lauri,
Sorry for the late reply.
Thanks for your enquire, please find answers below in “red”.
You want complete characterisation package similar to CCP-PKG1, but with ME-ICP06 replaced with ME-XRF24. In fact there is alternative CCP package CCP-PKG3, where whole rock analysis is done by XRF.
Adding F would cost 5.30 euro extra.
Best regards,
David
David Berglund
Senior Business Development Manager & Client Services Manager, Geochemistry
Nordic Region
T +46 911 658 00
M +46 70 608 61 10
[email protected] <mailto:
[email protected]>
Hammarvägen 22
SE-943 36 Piteå, Sweden
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From: Janette Mahony <
[email protected] <mailto:
[email protected]> >
Sent: Thursday, 12 November 2020 16:13
To: Lauri Joosu <
[email protected] <mailto:
[email protected]> >; David Berglund <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; Johannes Vind <
[email protected] <mailto:
[email protected]> >; Irene OMalley <
[email protected] <mailto:
[email protected]> >
Subject: RE: [EXTERNAL] - Phosphorite geochemical analysis information request.
Hi Lauri,
Thank you for your email. We received your web enquiry last Friday and my colleague David Berglund who is in copy here will assist you with your preparation and analytical requirements.
Kind Regards,
Jan
Janette Mahony
Executive Assistant & Office/Client Services Manager, Geochemistry
Ireland
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From: Lauri Joosu <
[email protected] <mailto:
[email protected]> >
Sent: 12 November 2020 10:12
To: Janette Mahony <
[email protected] <mailto:
[email protected]> >
Cc: Tiit Kaasik <
[email protected] <mailto:
[email protected]> >; Johannes Vind <
[email protected] <mailto:
[email protected]> >
Subject: [EXTERNAL] - Phosphorite geochemical analysis information request.
CAUTION: This email originated from outside of ALS. Do not click links or open attachments unless you recognize the sender and are sure content is relevant to you.
Dear Janette,
My name is Lauri Joosu and I’m writing to You from. The Geological Survey of Estonia. I have heard that you have been on contact with one of my college Johannes. We are working together with same deposit and while he is focusing on black shale my main target is phosphorite. Last week I made an inquiry (see below) in ALS website but I have not received any feedback. Maybe you can answer or forward this mail to correct person:
I’m looking laboratory to measure sedimentary phosphate ore chemical composition. For me it is important
• Major oxides, especially P2O5
• REE’s to understand if the deposit might have also REE potential
• Heavy metals (especially Cd and U)
• F as hazardous in ore processing technologies
Samples will be quatre of core so crushing prior analysis is also needed. Furthermore, all excess material must be shipped back to Estonia. I have about 100 samples with average weight about 4 kg per sample. I have selected from your list of services following packages:
1. PREP-31B
2. CCP-PKG01 but ME-ICP06 is replaced with ME-XRF24
3. Fluorine is measured by F-ELE81a
I have following questions:
• I did not find grain size distribution analysis from your service list. Do you provide this?
[David Berglund] We can perform this at our Metallurgy department in Australia.
• Please comment if my list of analysis is reasonable based on my expectations or would you recommend some changes.
[David Berglund] Se above.
• Please describe the difference in-between ME-ICP06 and ME-XRF24. I understood that for phosphorite study ME-XRF24 is recommended but I did not understand why.
[David Berglund] Main difference is in the analytical technique used. Decomposition is the same, correct – fusion with lithium borate. But in ICP06 fused bead is dissolved and measured by ICP-OES. In XRF26 the bead is cast on polished platinum mould and resulting disc is measured by XRF spectrometer – this method is much more precise.
• Please provide short standard operating procedure for each analyse package (what equipment used how calibrated etc).
I have understood that sample preparation is done in Finland and analysing in Ireland? How samples are shipped in-between laboratories?
[David Berglund] Yes, the sample preparation in this case is done at our lab in Outokumpu and after the sample preparation we are sending a small pulp-split by carrier to our hub-lab in Ireland for the analyses. Please find attached method descriptions.
• Please provide if and if are your laboratory has accredited for requested analyse sets. If you have please provided accreditation certificate.
[David Berglund] Please find attached.
• If inhouse blank’s and standard are used would you add this information report sheets upon request and provide certified values of standard that you have used.
[David Berglund] You will get a QQ/QC report when we report the assays where you can see our CRM´s used and the results.
• Please provide price estimate for analysis described below and rough estimate time of analyse (about 100 samples).
[David Berglund] If you think the method suggested are okay we will compose a quote for you.
Best Wishes,
Lauri Joosu
Senior Geologist
Mobile: +372 556 420 43
The Geological Survey of Estonia
https://www.egt.ee/en <https://aus01.safelinks.protection.outlook.com/?url=https%3A%2F%2Fwww.egt.ee%2Fen&data=04%7C01%7CDavid.Berglund%40alsglobal.com%7C9f63ad2c62154e39215008d9152c86ed%7C485ca04e6f7440509764cdb4bfa89c25%7C0%7C1%7C637564103910326096%7CUnknown%7CTWFpbGZsb3d8eyJWIjoiMC4wLjAwMDAiLCJQIjoiV2luMzIiLCJBTiI6Ik1haWwiLCJXVCI6Mn0%3D%7C1000&sdata=vVAlJa03UTzTX6nq88GA7BQM0t%2FFLGo1VC3CTVAo2Zw%3D&reserved=0>
ALS Finland Oy
Karjalankatu 1
FI-835 00 Outokumpu
FINLAND
T: +358 50 415 28 12
www.alsglobal.com
151 samples
List Price Discounted
ALS Minerals Per Sample Price Per
Description
Code (EUR) Sample
(EUR)
ADMINISTRATION
BAT-01 Processing fee for each batch of samples 39.75 39.75
submitted. per batch per batch
Webtrieve™ Personal username and password. Free of charge Free of charge
QA/QC Quality control of sample preparation including Free of charge Free of charge
preparation of duplicates. Analyses of internal
blanks, duplicates and standards.
SAMPLE PREPARATION
PREP-31Y Log sample in tracking system, barcode, weigh, 7.65 7.65
dry, fine crush entire sample to >70% passing + +
2mm, split off up to 250g with rotary split using 0.85/kg 0.85/kg
Boyd rotary splitter and pulverize split to >85%
passing 75 micron.
LOG-24 Log pulp sample (i.e. client standard) in tracking system, 1.40 1.40
barcode and weigh.
SHP-21 Labelling, packing and transport of a labsplit for by TBA 1.70
Express freight to ALS Geochemistry in Loughrea,
Ireland.
ANALYSIS
CCP-PKG03 Complete Characterization Package including the 83.90 75.50
following:
-- Whole rock analysis package (ME-XRF24) by
lithium borate fusion and XRF. LOI determination
must be done as part of the procedure.
-- Total C and Total S (ME-IR08), both 0.01-50%
by Leco furnace.
-- 30 trace elements, including the full rare earth
suite (Ba, Ce, Cr, Cs, Dy, Er, Eu, Ga, Gd, Hf, Ho,
La, Lu, Nb, Nd, Pr, Rb, Sm, Sn, Sr, Ta, Tb, Th,
Tm, U, V, W, Y, Yb, Zr) by lithium borate fusion
and ICP-MS (ME-MS81), for quantitative results of
all elements, including those encapsulated in
resistive minerals.
--Base metals(ME-4ACD81) by separate Four Acid
digestion and ICP-AES Finish, reported with ME-
MS81 method.
-- Volatile Au related trace elements (As, Bi, Hg,
Sb, Se, Te, Tl) by a separate aqua regia digestion
and ICP-MS analysis (ME-MS42). This digestion
quantitatively dissolves base metals for the
majority of geological materials.
Above prices are without VAT (VAT 0%) and are valid until 31st December 2021.
ALS-OT21-S008-The Geological Survey of Estonia-AIYEEG-Estonia
Quotation May 12th, 2021
RIGHT SOLUTIONS | RIGHT PARTNER
Sample Submittal Form Client Code:
INTERNAL USE ONLY
Workorder # Received Date Right Solutions • Right Partner
alsglobal.com
WORKORDER DETAILS SAMPLE AND ANALYSIS DETAILS
Company Name: Geological Survey of Estonia Sample Type: Overlimit Requirements: Special Instructions:
R-Rock SD-Sediment Report > no overlimit assay
1) Please weigh
Submitted by: Lauri Joosu
P-Pulp PC-Percussion Report via overlimit
crushed material
Contact Number: +37255642043 method (charges will
before returning
S-Soil DC-Drill core
apply)
(below 2 mm and
Courier/Waybill: DHL A-Solution (contact the lab) Other below 75 microns).
Other
Date Shipped: 19.05.2021 2) All samples must
be analysed in
Project ID: PandGA Phase Ia numeric order (see
PO Number: first column in
HAZARDOUS MATERIAL IDENTIFIED? (fees apply) Excel)
attatched
Dispatch #: 1 euro base
None Fibrous Radioactive Massive Sulphides Other:
ALS Quote #: ALS-OT21-S008
Sample ID Sample Preparation Analytical TYPE ORE
QTY
Start # Finish # (Prep Code) (Elements or Method Code) (R,S, etc.) GRADE
1 147 PREP-31Y CCP-PKG03 (XRF24+F) DC 147
148 152 PUL-31 CCP-PKG03 (XRF24+F) P 5
TOTAL 152
Check here for RUSH – PREMIUM SERVICE, CONTACT LAB TO CONFIRM AVAILABILITY SAMPLES
Webtrieve™
REPORTING DETAILS
Certificate
Data File
Invoice
# Name E-mail
1 Lauri Joosu on file
[email protected]
2 Tiit Kaasik on file
[email protected]
3 Johannes Vind on file
[email protected]
SAMPLE RESIDUE ARCHIVE AND RETURN DETAILS
All shipments received
IMMEDIATELY AFTER FREE STORAGE PERIOD* are subject to inspection
Sample Return
Return Discard Return Discard Paid storage upon layout; all services
Pulps – The <250g Master Pulp retained by the lab. are rendered in
accordance with ALS
Bulks – The remainder of large Pulp samples. Minerals Terms &
Conditions (see the
Rejects – Any remaining coarse unpulverised rejects. current Schedule of
Services & Fees).
Screen – Any screen reject fractions.
Return address: Arbavere küla, Kadrina vald45206 Lääne-Virumaa (Palkoja baas) * Free storage periods are: 45 days for coarse
rejects and bulk pulps, 90 days for Master
Attention: Inform L. Joosu atleast 2 days before returning the samples pulps and 45 days for screen reject fractions.
Authorised by:
Position Seniour geologist Name Lauri Joosu Signature
alsglobal.com/geochemistry